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20th August 2013 @ 14:15

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Reaction information

*#Reaction file
overallscheme_42.cdx
*Reaction file type CDX
*Procedure See child reaction steps 
*Yield (%)  
*Type of Yield  
Reference(s)
PhD Thesis - 16Sep2010_final p19.pdf
 
PhD Thesis - 16Sep2010_final p130-131.pdf
Further information Compound 42: 2,5-bis(2-(4-(Methylthio)phenyl)ethynyl)benzoic acid

For multistep reactions (or their steps):

Overall reaction? True
For overall reaction - links to child reaction steps

Reaction 21: Sonogashira Coupling: Trimethyl(2-(4-(methylthio)phenyl)ethynyl)silane

Reaction 39: Deprotection of trimethyl(2-(4-(methylthio)phenyl)ethynyl)silane: (4-ethynylphenyl)(methyl)sulfane

Reaction 40: Friedal-Crafts acylation: 2,5-dibromoacetophenone

Reaction 41: Oxidation of 2,5-dibromoacetophenone: 2,5-Dibromobenzoic acid

Reaction 42: Sonogashira coupling: 2,5-bis(2-(4-(methylthio)phenyl)ethynyl)benzoic acid

For step in multistep reaction - link to previous reaction step  
For step in multistep reaction - link to following reaction step  
Attached Files
overallscheme_42.cdx
PhD Thesis - 16Sep2010_final p19.pdf
PhD Thesis - 16Sep2010_final p130-131.pdf