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22nd August 2013 @ 10:18

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Reaction information

*#Reaction file  
CSRxnsScheme_102a.cdx
*Reaction file type CDX
*Procedure A solution of 3,5-dibenzyloxycytosoporone B (206 mg, 0.40 mmol) in ethanol (5.0 mL) was added dropwise to 5% Pd/C (85 mg, 0.04 mmol) and stirred at room temperature under hydrogen for 1 h.  The reaction mixture was filtered through celite and the solvent removed in vacuo to give the crude product as a white solid (124 mg). Purification by column chromatography (SiO2, hexane/Et2O 1:2) gave the title compound as a white solid (119 mg, 97%).
*Yield (%) 97
*Type of Yield Isolated product yield
Reference(s)  
AH Thesis_2011_pp168-175.pdf
AH Thesis_2011_pp71.pdf
Further information  Compound 102: Cytosporone B

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Overall reaction? True
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Attached Files
AH Thesis_2011_pp71.pdf
CSRxnsScheme_102a.cdx
AH Thesis_2011_pp168-175.pdf