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2nd September 2013 @ 10:59

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Reaction information

*#Reaction file
ReactionScheme.cdx
 
*Reaction file type CDX 
*Procedure A solution of 2-Phenyl-pent-4-en-1-ol (4.0 g, 25 mmol) in DCM (50 mL) was added to a stirred mixture of PCC (12.9 g, 60 mmol) on SiO2. After 5 hours the solution was poured nto a SiO2 column, eluted with 5 bed volumes of ether.
The crude product was purified by Kugelrohr distillation (90 °C, 0.5 mbar) and the columned (Al2O3, 10% ether in petrol) to provide the desired product.  
*Yield (%)
*Type of Yield -
Reference(s)

K. Omura, D. Swern, Tetrahedron 1978, 34, 1651.

Further information

The title compound was prepared by standard Swern oxidation conditions

Compound 326: 2-Phenyl-4-pentenal

For multistep reactions (or their steps):

Overall reaction? False 
For overall reaction - links to child reaction steps N/A 
For step in multistep reaction - link to previous reaction step Reaction 325 
For step in multistep reaction - link to following reaction step Reaction 327
Attached Files
ReactionScheme.gif
ReactionScheme.cdx
DavidOwenThesis2000pp48,49,116.pdf