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16th September 2013 @ 13:58

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Reaction information

*#Reaction file
ReactionScheme.cdx
 
*Reaction file type CDX 
*Procedure

To a stirred solution of tert-butyl 2-((3-(1-((3aR,6aR)-5-hexyl-4-phenyl-1,2,3,3a,6,6a-hexahydropentalen-3a-yl)vinyl)benzyl)oxy)acetate (95 mg, 0.18 mmol) in DCM (1.2 mL) was added TFA (0.3 mL) dropwise.  The reaction was stirred for 1 hour.

The reaction mixture was concentrated under reduced pressure and redissolved in chloroform before being concentrated again (a process that was repeated 3 times).  The crude product was used immediately in the next step of the synthesis.

*Yield (%) -
*Type of Yield -
Reference(s)
L.Sayerpp36-37.pdf
Further information

For multistep reactions (or their steps):

Overall reaction? False 
For overall reaction - links to child reaction steps N/A 
For step in multistep reaction - link to previous reaction step Reaction 69 
For step in multistep reaction - link to following reaction step Reaction 71
Attached Files
ReactionScheme.cdx
L.Sayerpp36-37.pdf